《化学和黏合》
 
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2018年 先后5希望

一个芳环堆积共结晶化合物的合成与表征
尹金城,王昌赫,王 莹,拉 磊**
(辽宁石油化工大学 化学和材料科学学院,辽宁 抚顺113001)
选择 如果:在溶剂中,使用水热法合成得到了一个旅结晶的花环堆积化合物C8H5O7S·C10H9N2·(C10H8N2)0.5(C10H8N2 = 2,2’-合并吡啶)。使用X射线单晶衍射和元素分析对那结构和整合进行了特点。X射线单晶衍射表征结果表明,该化合物晶体属于三斜晶系。研究了该化合物的荧光光谱以及热稳定性。该化合物荧光发射峰在417 nm。热稳定性较好。
关键词:花环堆积;共同结晶;特色
  受到图分类号:O625.7 文献标识码:A 文章编号:1001–0017 (2018)05–0334-03

Synthesis and Characterization of a Co-crystal Compound with Aromatic Ring Stacking

YIN Jin-cheng, WANG Chang-he, WANG Ying and GUAN Lei

(College of Chemistry and Materials Science, Liaoning University of Petroleum and Chemical Engineering, Fushun 113001, China)

Abstract: A co-crystal compound with aromatic ring stacking C8H5O7S·C10H9N2·(C10H8N2)0.5 (C10H8N2 = 2,2’-bipyridine) was synthesized by hydrothermal method in the solvent. The structure and composition were characterized by X-ray single crystal diffraction and elemental analysis. The result of X-ray single crystal diffraction showed that the compound belonged to the triclinic system. The fluorescence spectrum and thermal stability of the compound were investigated. The peak of the fluorescence emission of the compound was at 417 nm and the thermal stability was good.

Key words: Aromatic ring stacking; co-crystal; characterization

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